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The flux permeate and membrane durability were tested in preliminary experiments at different pressures and temperatures, vacuum pressure, water cooling temperature, and pervaporation time. Following two trial experiments, it was discovered that the geopolymer and Geo-TiO2NPs membranes exhibited significant cracking. Based on these findings, the pervaporation for all prepared membranes were conducted by adjusting the feed pressure to 2 psi, setting the feed temperatures to 40°, 60°, and 80 °C, a vacuum pressure of 0.75 bar, and a water-cooling temperature of 15 °C. Each set of experiments took about 5- 6 hours to complete in order to collect enough permeate for testing. Under the established pervaporation parameters, it was discovered that geopolymers and Geo-TiO2 (3) membranes still have significant cracks and thus reveal relatively high flux permeate, whereas Geo-rGO-TiO2 (0.5, 3) and Geo-rGO-TiO2 (1, 3) membranes had no surface cracks. As a result, the produced geopolymers and Geo-TiO2 (3) membranes are identified as being unable to withstand the feed's pressure and high temperature. The flux permeate of the membranes at various temperatures is depicted in Figure 5.
Response 7: Thank you for these questions. Our response has been added to the manuscript as follows. The measured TSS values of the membrane geopolymer and Geo-TiO2 (3) appear to be very high, exceeding the TSS value of seawater (feed). This value is unreasonable and is most likely due to the presence of alkali carbonate crystals detached from the surface and the cracks area of geopolymers and the Geo-TiO2 (3) membranes. One of the concerns with geopolymers made from metakaolin or fly ash is the formation of white needle-like alkali carbonate crystals known as efflorescence, which is caused by the mobility of excess alkali when the geopolymer is exposed to the open air or submerged in water for an extended period of time [26,27]. Despite the absence of surface cracks in the Geo-rGO-TiO2(0.5,1) and Geo-rGO-TiO2(1,5) membranes, NTU and TSS values are still high and detectable when NaCl rejection reaches 91%. Both membranes could also experience efflorescence, and in this case, the presence of high NTU and TSS values is due to the formation of alkaline carbonate crystals. More research is needed to confirm this.
Response 14: Thank you for this question. The statements in lines 269-272 were made based on our experimental results from a series of tests on Geo-rGO-TiO2 membranes. The results showed that incorporating rGO into the geopolymer paste has a significant impact on preventing cracks on the surface of the membranes. This finding is supported by other reports [18,38,39].
One of the concerns with geopolymers made from metakaolin or fly ash is the formation of white needle-like alkali carbonate crystals known as efflorescence, which is caused by the mobility of excess alkali when the geopolymer is exposed to the open air or submerged in water for an extended period of time [26,27]. Despite the absence of surface cracks in the Geo-rGO-TiO2(0.5,1) and Geo-rGO-TiO2(1,5) membranes, NTU and TSS values are still high and detectable when NaCl rejection reaches 91%. Both membranes could also experience efflorescence, and in this case, the presence of high NTU and TSS values is due to the formation of alkaline carbonate crystals. The efflorescence in geopolymer made from metakaolin can be controlled by adjusting the molar rasio of Na2O/Al2O3 of the alkali solution used [28], or the addition of soluble silicate, silica fume or silicone oil [29]. It is unclear whether the addition of rGO will be able to control the formation of efflorescence on the surface of the geopolymer. More research is needed to confirm this.
Response 6: This point is presumably connected to inquiry number 5. Until both membranes were removed from the membrane house once the level of permeate reached 1 liter, we were unaware that cracks were developing on the Geopolymer and Geo-TiO2 (3) membranes.
In our experiment, it was discovered that the Geo-rGO-TiO2NPS membranes were intact even after a lengthy working pervaporation time. Geopolymer membranes and Geo-TiO2(3), in contrast, show considerable cracks in a much shorter pervaporation time. This result reveals that the geopolymer paste surface cracks even at water pressures of roughly 2 psi, and that the cracking becomes worse at high feed temperatures.
Geopolymer is a heat- and temperature-resistant inorganic polymer that is widely used in construction. Even at 1000 oC, this material does not burn, although having significant cracks [4], [5]. The internal stress that the temperature will put on the geopolymer's structural element will cause cracks to start growing, as is well known. The strength of the pure geopolymer membrane will decrease as cracks develop. Adding graphene-based components like GO or rGO to geopolymers is one method used to increase their thermal strength [6].
Copyright © 2023 Yuan, Xiao, She, Zheng and Chen. This is an open-access article distributed under the terms of the Creative Commons Attribution License (CC BY). The use, distribution or reproduction in other forums is permitted, provided the original author(s) and the copyright owner(s) are credited and that the original publication in this journal is cited, in accordance with accepted academic practice. No use, distribution or reproduction is permitted which does not comply with these terms.
Copyright © 2023 Chen, Yang, Wang, Jiang and Ning. This is an open-access article distributed under the terms of the Creative Commons Attribution License (CC BY). The use, distribution or reproduction in other forums is permitted, provided the original author(s) and the copyright owner(s) are credited and that the original publication in this journal is cited, in accordance with accepted academic practice. No use, distribution or reproduction is permitted which does not comply with these terms. 2b1af7f3a8