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Download Nvidia TV Tuner TVP-AF90 driver software. free downloads .Structure characterization of acrylic acid/acrylic ester copolymer grafted with quaternized chitosan for oil-water separation.

Novel quaternized chitosan (QCS) was prepared by grafting acrylic acid and acrylic ester using maleic anhydride followed by epoxidation and quaternization. The structures of the grafted copolymers were characterized by (1)H NMR, FT-IR and gel permeation chromatography (GPC). The effects of the structure and Q-group on the separation characteristics of the QCS-g-AA/AE in oil-water separation were evaluated by oil absorption, emulsion stability and water permeability measurements. It was found that grafting AA and AE markedly enhanced the adsorption of oil by QCS and that the adsorption capacity of QCS-g-AA/AE was increased with increasing amounts of AA in the grafted copolymers. A special QCS-g-AA/AE with a high amount of AA grafted (35%) was studied for its potential application in oil-water separation by forming the emulsion formed by oil and water due to its high adsorption capacity of oil and its electrostatic repulsion on water surface. Experimental data showed that the adsorption and oil separation efficiencies of the QCS-g-AA/AE were significantly enhanced by the adsorption of the graft copolymer to the oil droplets of the emulsion formed. The GPC results showed that the average molecular weights of the polymer chains of QCS-g-AA/AE decreased when the ratio of acrylic acid to acrylonitrile in the grafted copolymers increased. The emulsion performance results showed that the QCS-g-AA/AE (35% of AA) with a high grafting density has the best performance. Water permeability results indicated that grafting AA/AE reduced the water permeability by reducing the water diffusion rate and molecular diffusion rate of the QCS-g-AA/AE. All of these results suggest that QCS-g-AA/AE could be a promising oil-water separation material.Q:

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